An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin

Dyeison Antonow; Cedric Stephan Graebin; Vera Lucia Eifler-Lima

doi:10.1590/S0103-50532004000500028

An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin

Dyeison Antonow
, Cedric Stephan Graebin
, Vera Lucia Eifler-Lima (Lead / Corresponding author)

Drug Discovery Unit

Research output: Contribution to journal › Article › peer-review

11 Citations (Scopus)

6 Downloads (Pure)

Abstract

The use of KBr pellets in infrared spectroscopy has been investigated for monitoring solid-phase reactions. Synthesis of the methyl p-aminobenzoate on Merrifield resin (MR) is described as a model for this technique, which allows the progress of its three on-bead reaction steps to be monitored throughout their duration.

Original language	English
Pages (from-to)	782-785
Number of pages	4
Journal	Journal of the Brazilian Chemical Society
Volume	15
Issue number	5
Early online date	10 Nov 2004
DOIs	https://doi.org/10.1590/S0103-50532004000500028
Publication status	Published - 2004

Keywords

Infrared spectroscopy
Merrifield resin
Microwave-assisted reactions
Solid phase organic synthesis

ASJC Scopus subject areas

General Chemistry

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10.1590/S0103-50532004000500028Licence: CC BY-NC

Final published versionFinal published version, 179 KBLicence: CC BY-NC

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title = "An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin",

abstract = "The use of KBr pellets in infrared spectroscopy has been investigated for monitoring solid-phase reactions. Synthesis of the methyl p-aminobenzoate on Merrifield resin (MR) is described as a model for this technique, which allows the progress of its three on-bead reaction steps to be monitored throughout their duration.",

keywords = "Infrared spectroscopy, Merrifield resin, Microwave-assisted reactions, Solid phase organic synthesis",

author = "Dyeison Antonow and Graebin, \{Cedric Stephan\} and Eifler-Lima, \{Vera Lucia\}",

year = "2004",

doi = "10.1590/S0103-50532004000500028",

language = "English",

volume = "15",

pages = "782--785",

number = "5",

}

An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin. / Antonow, Dyeison; Graebin, Cedric Stephan; Eifler-Lima, Vera Lucia (Lead / Corresponding author).
In: Journal of the Brazilian Chemical Society, Vol. 15, No. 5, 2004, p. 782-785.

Research output: Contribution to journal › Article › peer-review

TY - JOUR

T1 - An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin

AU - Antonow, Dyeison

AU - Graebin, Cedric Stephan

AU - Eifler-Lima, Vera Lucia

PY - 2004

Y1 - 2004

N2 - The use of KBr pellets in infrared spectroscopy has been investigated for monitoring solid-phase reactions. Synthesis of the methyl p-aminobenzoate on Merrifield resin (MR) is described as a model for this technique, which allows the progress of its three on-bead reaction steps to be monitored throughout their duration.

AB - The use of KBr pellets in infrared spectroscopy has been investigated for monitoring solid-phase reactions. Synthesis of the methyl p-aminobenzoate on Merrifield resin (MR) is described as a model for this technique, which allows the progress of its three on-bead reaction steps to be monitored throughout their duration.

KW - Infrared spectroscopy

KW - Merrifield resin

KW - Microwave-assisted reactions

KW - Solid phase organic synthesis

UR - https://www.scopus.com/pages/publications/9644275328

U2 - 10.1590/S0103-50532004000500028

DO - 10.1590/S0103-50532004000500028

M3 - Article

AN - SCOPUS:9644275328

SN - 0103-5053

VL - 15

SP - 782

EP - 785

JO - Journal of the Brazilian Chemical Society

JF - Journal of the Brazilian Chemical Society

IS - 5

ER -

An efficient monitoring technique for solid-phase reactions by KBr pellets/FT-IR using methyl p-aminobenzoate synthesis assisted by microwave radiation on Merrifield resin

Abstract

Keywords

ASJC Scopus subject areas

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