Rapid synthesis of hydroxyapatite nanopowders by a microwave-assisted combustion method

Nagmeh Bovand, Sousan Rasouli, Mohammad Reza Mohammadi, Davood Bovand

    Research output: Contribution to journalArticlepeer-review

    6 Citations (Scopus)

    Abstract

    Nano bioactive hydroxyapatite (Ca 10(PO 4) 6(OH) 2, HAp) ceramic powders have been synthesized by a microwave-assisted combustion method. The powders were synthesized using calcium nitrate tetrahydrate (as the source of calcium) and sodium phosphate dibasic anhydrous (as the source of phosphate ions). Glycine, citric acid and urea were used as fuesl. The influence of the fuel type on the structure and morphology of the samples was studied. Results by X-ray diffraction and Fourier-transform infrared spectroscopy showed the formation of hydroxyapatite as a major phase for all the samples. Using the Scherrer formula, the average crystallite size was found to be in the range of 10 to 28 nm. SEM-EDX results showed highly crystalline nano-powders with an elemental composition of Ca and P in the HAp phase. The morphology of the particles was dependent an the fuel type and changed from semi-spherical to elongated. Smaller particles were obtained with glycine as the fuel.

    Original languageEnglish
    Pages (from-to)221-225
    Number of pages5
    JournalJournal of Ceramic Processing Research
    Volume13
    Issue number3
    Publication statusPublished - 19 Jul 2012

    Keywords

    • Combustion synthesis
    • Fuel
    • Hydroxyapatite
    • Morphology

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