SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

Christine Edwards; Craig McKenzie; Carlos Joao  Pestana; Kyari   Yates; Linda A.  Lawton

doi:10.1002/9781119068761.ch60

SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

Christine Edwards, Craig McKenzie, Carlos Joao Pestana, Kyari Yates, Linda A. Lawton

Centre for Anatomy and Human Identification

Research output: Chapter in Book/Report/Conference proceeding › Chapter (peer-reviewed) › peer-review

Abstract

This procedure is a simple and robust method of extracting and analysing the problematic taste and odour compounds, geosmin (GSM) and 2-methylisoborneol (2-MIB), from water sampled from surface and drinking water sources. The use of solid-phase extraction (SPE) for extraction facilitates high throughput clean-up and concentration of GSM and 2-MIB in diverse water samples. In addition to simplicity, this approach offers an option of remote sampling, shipping, and analysis. Elution of the SPE cartridge is followed by established GC-MS analysis. This method was successfully applied for investigating the destruction of GSM and 2-MIB in a continuous packed bed photocatalytic reactor.

Original language	English
Title of host publication	Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis
Editors	Jussi Meriluoto, Lisa Spoof, Geoffrey A. Codd
Publisher	John Wiley & Sons Inc.
Pages	475-480
Number of pages	6
ISBN (Electronic)	9781119068761
ISBN (Print)	9781119068686
DOIs	https://doi.org/10.1002/9781119068761.ch60
Publication status	Published - 2017

Keywords

Taste
Odour
Geosmin
2-methylisoborneol
SPE
GC-MS

UN SDGs

This output contributes to the following UN Sustainable Development Goals (SDGs)

Access to Document

10.1002/9781119068761.ch60

Cite this

Edwards, C., McKenzie, C., Pestana, C. J., Yates, K., & Lawton, L. A. (2017). SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS. In J. Meriluoto, L. Spoof, & G. A. Codd (Eds.), Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis (pp. 475-480). John Wiley & Sons Inc.. https://doi.org/10.1002/9781119068761.ch60

@inbook{59fe0d174f0a4b358142880761e6aefd,

title = "SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS",

abstract = "This procedure is a simple and robust method of extracting and analysing the problematic taste and odour compounds, geosmin (GSM) and 2-methylisoborneol (2-MIB), from water sampled from surface and drinking water sources. The use of solid-phase extraction (SPE) for extraction facilitates high throughput clean-up and concentration of GSM and 2-MIB in diverse water samples. In addition to simplicity, this approach offers an option of remote sampling, shipping, and analysis. Elution of the SPE cartridge is followed by established GC-MS analysis. This method was successfully applied for investigating the destruction of GSM and 2-MIB in a continuous packed bed photocatalytic reactor.",

keywords = "Taste , Odour, Geosmin , 2-methylisoborneol , SPE , GC-MS",

author = "Christine Edwards and Craig McKenzie and Pestana, {Carlos Joao} and Kyari Yates and Lawton, {Linda A.}",

note = "No funding info",

year = "2017",

doi = "10.1002/9781119068761.ch60",

language = "English",

isbn = "9781119068686",

pages = "475--480",

editor = "Meriluoto, {Jussi } and Spoof, {Lisa } and Codd, { Geoffrey A.}",

booktitle = "Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis",

publisher = "John Wiley & Sons Inc.",

address = "United States",

}

SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS. / Edwards, Christine; McKenzie, Craig; Pestana, Carlos Joao et al.

Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis. ed. / Jussi Meriluoto; Lisa Spoof; Geoffrey A. Codd. John Wiley & Sons Inc., 2017. p. 475-480.

Research output: Chapter in Book/Report/Conference proceeding › Chapter (peer-reviewed) › peer-review

TY - CHAP

T1 - SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

AU - Edwards, Christine

AU - McKenzie, Craig

AU - Pestana, Carlos Joao

AU - Yates, Kyari

AU - Lawton, Linda A.

N1 - No funding info

PY - 2017

Y1 - 2017

N2 - This procedure is a simple and robust method of extracting and analysing the problematic taste and odour compounds, geosmin (GSM) and 2-methylisoborneol (2-MIB), from water sampled from surface and drinking water sources. The use of solid-phase extraction (SPE) for extraction facilitates high throughput clean-up and concentration of GSM and 2-MIB in diverse water samples. In addition to simplicity, this approach offers an option of remote sampling, shipping, and analysis. Elution of the SPE cartridge is followed by established GC-MS analysis. This method was successfully applied for investigating the destruction of GSM and 2-MIB in a continuous packed bed photocatalytic reactor.

AB - This procedure is a simple and robust method of extracting and analysing the problematic taste and odour compounds, geosmin (GSM) and 2-methylisoborneol (2-MIB), from water sampled from surface and drinking water sources. The use of solid-phase extraction (SPE) for extraction facilitates high throughput clean-up and concentration of GSM and 2-MIB in diverse water samples. In addition to simplicity, this approach offers an option of remote sampling, shipping, and analysis. Elution of the SPE cartridge is followed by established GC-MS analysis. This method was successfully applied for investigating the destruction of GSM and 2-MIB in a continuous packed bed photocatalytic reactor.

KW - Taste

KW - Odour

KW - Geosmin

KW - 2-methylisoborneol

KW - SPE

KW - GC-MS

UR - https://www.wiley.com/en-gb/Handbook+of+Cyanobacterial+Monitoring+and+Cyanotoxin+Analysis-p-9781119068747

U2 - 10.1002/9781119068761.ch60

DO - 10.1002/9781119068761.ch60

M3 - Chapter (peer-reviewed)

SN - 9781119068686

SP - 475

EP - 480

BT - Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis

A2 - Meriluoto, Jussi

A2 - Spoof, Lisa

A2 - Codd, Geoffrey A.

PB - John Wiley & Sons Inc.

ER -

SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

Abstract

Keywords

UN SDGs

Access to Document

Other files and links

Fingerprint

McKenzie, Craig

Cite this

SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

Abstract

Keywords

UN SDGs

Access to Document

Other files and links

Fingerprint

Profiles

McKenzie, Craig

Cite this