SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

Christine Edwards; Craig McKenzie; Carlos Joao  Pestana; Kyari   Yates; Linda A.  Lawton

doi:10.1002/9781119068761.ch60

SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS

Christine Edwards, Craig McKenzie, Carlos Joao Pestana, Kyari Yates, Linda A. Lawton

Centre for Anatomy and Human Identification

Research output: Chapter in Book/Report/Conference proceeding › Chapter (peer-reviewed) › peer-review

Abstract

This procedure is a simple and robust method of extracting and analysing the problematic taste and odour compounds, geosmin (GSM) and 2-methylisoborneol (2-MIB), from water sampled from surface and drinking water sources. The use of solid-phase extraction (SPE) for extraction facilitates high throughput clean-up and concentration of GSM and 2-MIB in diverse water samples. In addition to simplicity, this approach offers an option of remote sampling, shipping, and analysis. Elution of the SPE cartridge is followed by established GC-MS analysis. This method was successfully applied for investigating the destruction of GSM and 2-MIB in a continuous packed bed photocatalytic reactor.

Original language	English
Title of host publication	Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis
Editors	Jussi Meriluoto, Lisa Spoof, Geoffrey A. Codd
Publisher	John Wiley & Sons Inc.
Pages	475-480
Number of pages	6
ISBN (Electronic)	9781119068761
ISBN (Print)	9781119068686
DOIs	https://doi.org/10.1002/9781119068761.ch60
Publication status	Published - 2017

Keywords

Taste
Odour
Geosmin
2-methylisoborneol
SPE
GC-MS

Access to Document

10.1002/9781119068761.ch60

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McKenzie, Craig
- Leverhulme Research Centre for Forensic Science - Senior Lecturer (Teaching and Research)
Person: Academic

Cite this

Edwards, C., McKenzie, C., Pestana, C. J., Yates, K., & Lawton, L. A. (2017). SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS. In J. Meriluoto, L. Spoof, & G. A. Codd (Eds.), Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis (pp. 475-480). John Wiley & Sons Inc.. https://doi.org/10.1002/9781119068761.ch60

Edwards, Christine ; McKenzie, Craig ; Pestana, Carlos Joao ; Yates, Kyari ; Lawton, Linda A. . / SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS. Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis. editor / Jussi Meriluoto ; Lisa Spoof ; Geoffrey A. Codd. John Wiley & Sons Inc., 2017. pp. 475-480

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abstract = "This procedure is a simple and robust method of extracting and analysing the problematic taste and odour compounds, geosmin (GSM) and 2-methylisoborneol (2-MIB), from water sampled from surface and drinking water sources. The use of solid-phase extraction (SPE) for extraction facilitates high throughput clean-up and concentration of GSM and 2-MIB in diverse water samples. In addition to simplicity, this approach offers an option of remote sampling, shipping, and analysis. Elution of the SPE cartridge is followed by established GC-MS analysis. This method was successfully applied for investigating the destruction of GSM and 2-MIB in a continuous packed bed photocatalytic reactor.",

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author = "Christine Edwards and Craig McKenzie and Pestana, {Carlos Joao} and Kyari Yates and Lawton, {Linda A.}",

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SOP 28. Rapid Analysis of Geosmin and 2-Methylisoborneol from Aqueous Samples Using Solid-Phase Extraction and GC-MS. / Edwards, Christine; McKenzie, Craig; Pestana, Carlos Joao ; Yates, Kyari ; Lawton, Linda A. .

Handbook of Cyanobacterial Monitoring and Cyanotoxin Analysis. ed. / Jussi Meriluoto; Lisa Spoof; Geoffrey A. Codd. John Wiley & Sons Inc., 2017. p. 475-480.

Research output: Chapter in Book/Report/Conference proceeding › Chapter (peer-reviewed) › peer-review

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KW - 2-methylisoborneol

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